| 标题 |
[高分] The substrates 3, 5, and 7 were prepared starting from the corresponding allylic alcohols by the sequence: 1) conversion into chloroformates by reaction with phosgene, 2) treatment of the chloroformates with o-aminobenzyl alcohol, and 3) conversion of the resulting hydroxy carbamates into the corresponding chlorides with thionyl chloride (see experimental section for details). 3-Chloro-2-methyl-2- propen-1-ol was prepared according to A
底物3、5和7从相应的烯丙醇开始按照以下顺序制备：1)通过与光气反应转化为氯甲酸酯，2)用邻氨基苄醇处理氯甲酸酯，和3)用亚硫酰氯将所得羟基氨基甲酸酯转化为相应的氯化物(详情参见实验部分)。3-氯-2-甲基-2-丙烯-1-醇
|
| 网址 |
求助人暂未提供
|
| DOI |
暂未提供，该求助的时间将会延长，查看原因？
|
| 其它 |
Mooradian, J. B. Cloke, J.Am. Chem. Soc. 1946, 68, 785 ± 789; L. F. Hatch, J. J. Russ, L. B.Gordon, J. Am. Chem. Soc. 1947, 69, 2614 ± 2616. Enantiomericallypure (R)-2-cyclohexen-1-ol was prepared by kinetic resolution with lipase as described by T. Fukazawa, T. Hashimoto, Tetrahedron:Asymmetry 1993, 4, 2323 ± 2326. |
| 求助人 | |
| 下载 | 该求助完结已超 24 小时，文件已从服务器自动删除，无法下载。 |
劲秉
cdercder
科研小民工
科研321
昏睡的蟠桃
pluto
随遇而安
back you up
HEIKU
子车茗
默默地读文献
iNk
迷人秋烟
Thien
chunjuan
yoyofun
YifanWang
罗_
xiaxiao
实验好难
皖公网安备34019202002308
