| 标题 |
 Determination of glyphosate and its metabolite,(aminomethyl) phosphonic acid, in serum using capillary electrophoresis 毛细管电泳法测定血清中草甘膦及其代谢产物（氨甲基）膦酸
相关领域
化学
毛细管电泳
色谱法
代谢物
衍生化
氨基甲基膦酸
检出限
氢氧化钠
草甘膦
硼酸
甲醇
钠
高效液相色谱法
生物化学
有机化学
农学
生物
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| 其它 |
M Tomita, T Okuyama, Y Nigo, B Uno… - Journal of Chromatography …, 1991 - Elsevier Capillary electrophoresis has been used to separate and quantitate glyphosate and its major metabolite,(aminomethyl) phosphonic acid (AMPA), in serum. The two compounds, after derivatization with p-toluenesulphonyl chloride, were clearly separated with 0.1 M boric acid—sodium hydroxide buffer (pH 9.6) containing 10% methanol. The separation was completed within 15 min at an applied potential of 30 kV. Calibration curves for the assay were linear over both the lower (0.5–10 μg/ml) and the higher (10–100 μg/ml) concentration |
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