聚碳酸酯
三光气
材料科学
粘度计
粘度
原材料
缩聚物
聚合物
热塑性塑料
复合材料
高分子化学
化学工程
有机化学
化学
工程类
光气
作者
E Yongsheng,Ping Lv,Fang Yang
出处
期刊:Journal of physics
[IOP Publishing]
日期:2022-02-01
卷期号:2194 (1): 012033-012033
标识
DOI:10.1088/1742-6596/2194/1/012033
摘要
Abstract Polycarbonate is a widely used thermoplastic engineering plastic with excellent properties. Using triphosgene and Bisphenol A as raw materials, polycarbonate is synthesized by interfacial polycondensation. The effects of catalyst dosage, molar ratio of raw material, reaction temperature and reaction time on the molecular weight of the product are investigated, and the optimal reaction conditions are obtained. The structure of the product is verified by infrared absorption spectroscopy. The rotary viscometer measures the intrinsic viscosity of the sample and calculates the viscosity average molecular weight of the sample to be 50000. The glass transition temperature of the product is detected to be 148.5 °C by dilatometer. The polycarbonate synthesized by the new method meets the quality requirements.
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