非阻塞I/O
材料科学
煅烧
氧化镍
化学工程
氢
旋涂
薄膜
氢传感器
多孔性
氧化物
纳米技术
分析化学(期刊)
冶金
复合材料
催化作用
钯
生物化学
化学
有机化学
色谱法
工程类
作者
Shri Hari S. Pai,Anibrata Mondal,Ramya Barathy T,B. Ajitha,E. James Jebaseelan Samuel,Y. Ashok Kumar Reddy
标识
DOI:10.1016/j.ijhydene.2023.07.345
摘要
In this work, we have synthesized the nickel oxide (NiO) nanopowders via twofold facile solvothermal synthesis. Later, the products are calcined at 300 °C, 400 °C, and 500 °C in an air atmosphere to form NiO nanopowders, which are deposited onto the SiO2/Si substrate via the spin coating technique. The morphological studies depict the high porosity at 400 °C calcinated NiO thin film than other conditions. Further, the Brunauer-Emmett-Teller (BET) surface analysis reveals that at 400 °C calcinated NiO sample exhibits a higher surface area of 52.3 m2g-1 due to the existence of porous grain-like surface morphology. To examine the gas sensing performance, Ag/NiO/Ag hydrogen gas sensor device is fabricated by depositing planar-type silver (Ag) electrodes onto the NiO thin film via thermal evaporation technique. The gas sensing behaviour of the fabricated gas sensor test-devices has been examined at various operating temperatures (100 °C–300 °C) and concentrations (100 ppm–300 ppm). The hydrogen gas sensor test-device fabricated using NiO nanopowder calcined at 400 °C shows good crystalline nature, a highly porous surface with efficient oxygen vacancies, and narrowed bandgap, which results in the maximum responsivity of 97.2% at the operating temperature of 250 °C with response and recovery time of 56 s and 21 s, respectively. Therefore, the Ag/NiO/Ag gas sensor test-device can be a potential route toward the development of hydrogen gas sensor devices.
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