材料科学
微观结构
合金
维氏硬度试验
差示扫描量热法
光学显微镜
透射电子显微镜
冶金
硬化(计算)
压痕硬度
金属间化合物
沉淀硬化
扫描电子显微镜
复合材料
图层(电子)
物理
纳米技术
热力学
作者
Fellipe Martinez,Carlos Alexandre dos Santos,Jaderson Leal,Argos Silva,Guilherme Pertinni de Morais Gouveia,José Eduardo Spinelli
标识
DOI:10.1002/adem.202300596
摘要
Cu‐mold centrifugal cast processing is employed as a rapid solidification method for producing samples with and without Sc. The Al–Si–Mg and Al–Si–Mg–Sc alloy samples are exposed to direct aging treatments varying temperature and time to verify the microstructural changes. Both rapidly solidified samples and as‐aged samples are characterized by a number of methods, including optical microscopy, SEM–EDS, transmission Electron Microscopy (TEM)–EDS, TEM–HAADF, X‐ray diffraction (XRD), differential scanning calorimetry (DSC), and Vickers hardness. At first, the results point to a strong precipitate‐related hardening effect formed as a result of the Sc addition to the alloy. All samples containing Sc show a higher hardness value when compared to their respective treated samples without Sc. Second, when comparing the Al–10Si–Mg–0.4Sc alloy samples among themselves after being treated at different conditions, high temperatures, and excessive treatment times are recognized as detrimental to the hardness. This is due to the growth of larger Sc‐bearing precipitates of approximately 1 μm in size under such conditions, having lower efficiency in pinning dislocations during loading. The best aging condition is 255 °C for 60 min, which produces a very fine dispersion of Mg and Sc intermetallics (200 nm in size) with a peak hardness of 110 HV.
科研通智能强力驱动
Strongly Powered by AbleSci AI