A Remarkably Simple One-Step Procedure for the Preparation of α-Bromo-α,β-Unsaturated Carbonyl Compounds
化学
二氯甲烷
碳酸钾
钾
有机化学
溶剂
作者
Divya Jyothi,S. A. Hariprasad
出处
期刊:Synlett [Thieme Medical Publishers (Germany)] 日期:2009-08-03卷期号:2009 (14): 2309-2311被引量:7
标识
DOI:10.1055/s-0029-1217726
摘要
An easy and convenient one-step procedure for the conversion of α,β-unsaturated carbonyl compounds into their corresponding bromo-enones using NBS-Et3N˙3HBr in the presence of potassium carbonate in dichloromethane at 0 ˚C to room temperature under very mild conditions in high yields and significantly shorter times, is reported.