东莨菪碱
化学
石油醚
伞形酮
硅胶
乙酸乙酯
色谱法
氯仿
柱色谱法
补骨脂素
甲醇
乙醚
有机化学
香豆素
萃取(化学)
生物化学
替代医学
DNA
病理
医学
作者
Wen Li,Shilan Feng,Fangdi Hu,Erlin Chen
摘要
The root of Peucedanum harry-smithii var. subglabrum was extracted with methanol, then separated with solvents at different polarity into four fractions: aqueous (H2O), ethyl acetate (AcOEt), chloroform (CHCl3) and petroleum ether (DAB-6). From AcOEt psoralen, bargapten, xanthotoxin, marmesin, umbelliferone, scopoletin, (+/-) peuformosin, Pd-I b, (+/-) selinidin, praeruptorin D were isolated by column chromatography on silica gel, using petroleum ether/ethyl acetate as eluent. The structures of the coumarins were identified by 1H-NMR and 13C-NMR.
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