Low temperature growth of vanadium pentoxide nanomaterials by chemical vapour deposition using VO(acac)2as precursor

五氧化二铁 过饱和度 化学气相沉积 纳米线 纳米材料 材料科学 蒸发 拉曼光谱 扫描电子显微镜 化学工程 分析化学(期刊) 化学 纳米技术 有机化学 冶金 物理 工程类 光学 复合材料 热力学
作者
Y Wang,Qing Su,C H Chen,Minglang Yu,Guankai Han,G Q Wang,Ke Ke Xin,Wen Lan,Dage Liu
出处
期刊:Journal of Physics D [IOP Publishing]
卷期号:43 (18): 185102-185102 被引量:41
标识
DOI:10.1088/0022-3727/43/18/185102
摘要

Vanadium pentoxide (V2O5) nanomaterials with various morphologies were prepared by chemical vapour deposition at a relatively low temperature (evaporation temperature of 250 °C and growth temperature of 500 °C) using vanadyl acetylacetonate (VO(acac)2) powder as the vanadium precursor. The obtained samples were characterized by scanning electron microscopy, x-ray diffraction, Raman scattering and photoluminescence spectra. The results revealed that the samples including a V2O5 nanocluster film, V2O5 nanowires and V2O5 nanospheres were synthesized at different distances from the source material. For our chemical vapour transport system, we suggested that VOx vapour and VO(acac)2 vapour existed simultaneously during the growth process, which resulted in different morphologies of V2O5 nanomaterials. The quite different supersaturation distributions of VOx vapour and VO(acac)2 vapour led to three main growth areas. The V2O5 film was grown in the region where the supersaturation of the VOx vapour was high, V2O5 nanowires were obtained where the supersaturation of the VOx vapour was relatively low and V2O5 nanospheres were synthesized in the region where the supersaturation of the VO(acac)2 vapour was high. The growth pressure that influenced the vapour concentration controlled the morphologies of the nanowires. It was found that a specific level of low concentration was necessary to ensure the growth of V2O5 nanowires.

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