Convenient Method for the Preparation of Heterodialkyl‐H‐phosphonates from Diphenyl‐H‐phosphonate

Abstract A procedure for the introduction of two different alkyl chains (myristyl, oleyl and phytanyl) leading to heterodialkyl‐H‐phosphonates is reported, based on two successive transesterification reactions of commercially available diphenyl‐H‐phosphonate with the corresponding alcohols.