Synthesis and characterization of copper oxide nanocrystal via preparation of precursor tri-homo-nuclear inorganic complex

In this investigation, we report synthesis of new trinuclear complex of Copper under formula [(phen)2(H2O)Cu(µ-NCS)Cu(NCS)4(µ-SCN)Cu(OH2)(phen)2]Cl2(1) that phen = 1–10 phenanthroline. This complex has been characterized using FT-IR, UV–Vis, Conductivity and Cyclic voltammetry (CV) techniques. Also in this study we report facile synthesis of Copper Oxide nanocomposite under thermal decomposition, using synthesize precursor complex. Characterization of Copper nanocompound was carried out by scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX), X-ray powder diffraction (XRD) and Fourier transform infrared (FT-IR) spectroscopy. Also magnetic behavior of nanoparticle characterized using VSM technique. The X-ray diffraction pattern at room temperature revealed, highly pure system CuO with monoclinic structure.