煅烧
化学工程
材料科学
水溶液
氧化物
复合数
纳米颗粒
氢氧化物
催化作用
纳米技术
铁
金属
化学
复合材料
冶金
有机化学
工程类
作者
В. И. Михайлов,Elena F. Krivoshapkina,В. А. Белый,Pavel V. Krivoshapkin
标识
DOI:10.1016/j.ces.2017.01.025
摘要
Sponge-like magnetic α-Fe microtubes have been prepared via reduction of α-Fe2O3 microtubes in hydrogen flow. α-Fe2O3 microtubes have been previously obtained by combined sol-gel and template methods. It is shown that the strongly acidic aqueous medium leads to specific interaction of ferric hydroxide nanoparticles with cellulose template. This contributes to the formation of α-Fe2O3 microtubes, which retain the features of the initial fibers structure. Both calcination at high temperature (1200 °C) and reduction does not lead to the destruction of the tubular morphology. The resulting magnetic materials have a promising applications in biomedicine, as micro-reactors, microwave absorbing materials, easily recoverable from the reaction medium catalysts of various chemical reactions (including carbon nanotubes growth) and a component for creating new composite (e.g., metal-oxide) materials with improved performance characteristics.
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