涂层
材料科学
浸涂
接触角
复合材料
聚乳酸
表面粗糙度
管(容器)
聚合物
作者
Mariana Macías-Naranjo,Margarita Sánchez‐Domínguez,José Fernando Rubio‐Valle,Ciro A. Rodrı́guez,J.E. Martín‐Alfonso,Erika García‐López,Elisa Vázquez
出处
期刊:Polymers
[MDPI AG]
日期:2024-01-19
卷期号:16 (2): 284-284
被引量:2
标识
DOI:10.3390/polym16020284
摘要
The dip coating process is one of the recognized techniques used to generate polymeric coatings on stents in an easy and low-cost way. However, there is a lack of information about the influence of the process parameters of this technique on complex geometries such as stents. This paper studies the dip coating process parameters used to provide a uniform coating of PLA with a 4–10 µm thickness. A stainless-steel tube (AISI 316L) was laser-cut, electropolished, and dip-coated in a polylactic acid (PLA) solution whilst changing the process parameters. The samples were characterized to examine the coating’s uniformity, thickness, surface roughness, weight, and chemical composition. FTIR and Raman investigations indicated the presence of PLA on the stent’s surface, the chemical stability of PLA during the coating process, and the absence of residual chloroform in the coatings. Additionally, the water contact angle was measured to determine the hydrophilicity of the coating. Our results indicate that, when using entry and withdrawal speeds of 500 mm min−1 and a 15 s immersion time, a uniform coating thickness was achieved throughout the tube and in the stent with an average thickness of 7.8 µm.
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