苋菜
硬脂酸
苋菜
极限抗拉强度
甘油
增塑剂
溶解度
材料科学
透氧性
乳状液
延伸率
化学
响应面法
化学工程
核化学
复合材料
色谱法
食品科学
氧气
有机化学
工程类
作者
Eliane Colla,Paulo José do Amaral Sobral,Florência Cecília Menegalli
摘要
Films forming solutions composed of Amaranth (Amaranthus cruentus) flour (4.0 g/100 mL), stearic acid (5−15 g/100 g of flour), and glycerol (25−35 g/100 g of flour) were prepared by an emulsification process, with varying stirring speed values (6640−13360 rpm). The influence of these parameters (stearic acid and glycerol concentrations and stirring speed) on the water vapor barrier and mechanical properties of films was evaluated using the response surface methodology (RSM). Other characterizations, including microstructure, water solubility, and oxygen permeability, were performed in optimized films. According to statistical analysis results, the optimized conditions corresponded to 10 g of stearic acid/100 g of flour, 26 g of glycerol/100 g of flour, and a stirring speed of 12 000 rpm. The films produced under these conditions exhibited superior mechanical properties (2.5 N puncture force, 2.6 MPa tensile strength, and 148% elongation at break) in comparison to those of other protein and polysaccharide composite films, low solubility (15.2%), and optimal barrier properties (WVP of 8.9 × 10-11 g m-1 s-1 Pa-1 and oxygen permeability of 2.36 × 10-13 cm3 m-1 s-1 Pa-1). Keywords: Edible films; Amaranthus cruentus; lipids; mechanical properties; water vapor permeability
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