X射线光电子能谱
扫描电子显微镜
电镀(地质)
材料科学
表面改性
镍
纤维
碳纤维
形态学(生物学)
化学工程
沉积(地质)
图层(电子)
复合材料
冶金
复合数
古生物学
工程类
地质学
生物
遗传学
地球物理学
沉积物
作者
Qinghui Wang,Xuesong Li,Dongdong Zhu
出处
期刊:Materials
[MDPI AG]
日期:2024-07-24
卷期号:17 (15): 3650-3650
摘要
This study explores the effects of various temperatures on the surface modification of carbon fibers, as well as the effect of differing voltages and currents on the morphology, deposition rate, and thickness of the Ni plating layers. Post-treatment characterization of the samples was conducted utilizing scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS) methods, thus facilitating a discussion on the mechanism of Ni plating. The findings demonstrate that at a temperature of 500 °C, the carbon fiber surface exhibits the highest concentration of functional groups, including hydroxyl (-OH), carboxyl (-COOH), and carbonyl (-C=O), resulting in the most efficacious modification. Specifically, exceeding 500 °C leads to significant carbon fiber mass loss, compromising the reinforcement effect. Under a stable voltage of 7.5 V, the Ni-plated layer on the carbon fibers appear smooth, fine, uniform, and complete. Conversely, at a voltage of 15 V, the instantaneous high voltage induces the continuous growth of Ni2+ ions along a singular deposition point, forming a spherical Ni-plated layer. In addition, a current of 0.6 A yields a comparatively uniform and dense carbon fiber coating. Nickel-plated layers on a carbon fiber surface with different morphologies have certain innovative significance for the structural design of composite reinforcements.
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