差示扫描量热法                        
                
                                
                        
                            结晶度                        
                
                                
                        
                            傅里叶变换红外光谱                        
                
                                
                        
                            材料科学                        
                
                                
                        
                            喷雾干燥                        
                
                                
                        
                            粒径                        
                
                                
                        
                            化学工程                        
                
                                
                        
                            复合材料                        
                
                                
                        
                            化学                        
                
                                
                        
                            色谱法                        
                
                                
                        
                            物理化学                        
                
                                
                        
                            物理                        
                
                                
                        
                            工程类                        
                
                                
                        
                            热力学                        
                
                        
                    
            作者
            
                Xinhua Wang,Xiaojing Tian,Qiuli Wang,Ruixi Shen,Chenwei Ma,Lei Bai,Wenhang Wang            
         
                    
        
    
            
            标识
            
                                    DOI:10.1016/j.jfoodeng.2023.111773
                                    
                                
                                 
         
        
                
            摘要
            
            In this study, a new and efficient method combining microwave and hot-air drying was developed to prepare collagen fiber powder (CFP) from cowhide. The cowhide was first dried to a certain humidity by microwave, and then dried under different hot-air treatment times (6 h, 12 h, 18 h, 24 h, 48 h). The physicochemical and functional properties of CFP were evaluated. The results indicated that extending the hot-air drying time increased the crushing rate and decreased the particle size of CFP. Ostwald de Waele model analysis showed that CFP solution was a typical pseudo-plastic fluid with shear-thinning behavior. Moreover, X-ray diffraction (XRD) and differential scanning calorimetry (DSC) analysis showed that the crystallinity and thermal stability of CFP decreased with the extension extending of drying time. In addition, the hydrogen bond content of CFP decreased by fourier transform infrared spectroscopy (FTIR) and secondary structure analysis, and the ordered structure of collagen changed into disordered structure gradually.
         
            
 
                 
                
                    
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