In-situ SEM study on fatigue crack behavior of a nickel-based single crystal alloy at 950 °C and 1050 °C

As the blade material of engine, nickel-base single crystal superalloy has been subjected to complex service environment such as high temperature and alternating load for a long time. In this work, the mechanism of fatigue microcrack initiation and propagation in a nickel-based single crystal at 950 °C and 1050 °C was studied by using the in-situ scanning electron microscope high temperature fatigue test system. At 950 °C, the alloy deformation was controlled by slip and the crack shear γ/γ' phase cracking, showing Stage I mode. At 1050 °C, the alloy crack tearing occurred at the γ phase parallel to the loading direction and γ/γ' interface perpendicular to the loading direction and presents a Stage II mode perpendicular to the loading axis, then changes into Stage I in the accelerating stage. The deformation mechanism of fatigue cracking at two temperatures was compared. Besides, the influence of the microstructure defects on the fatigue crack behavior was discussed. The results show that the propagation of the microcrack below 100 μm shows evident fluctuations, which is closely related to the microstructure and the development stage of the fatigue crack.