Investigation of aerosol droplets diameter generated in aerosol jet printing

气溶胶 材料科学 扫描电子显微镜 喷射(流体) 粘度 墨水池 复合材料 沉积(地质) 聚对苯二甲酸乙二醇酯 箔法 纳米技术 分析化学(期刊) 化学 色谱法 古生物学 物理 有机化学 沉积物 生物 热力学
作者
Wojciech Łapa,Marcin Winnicki,Karolina Orłowska
出处
期刊:Materials Science Poland [De Gruyter Open]
卷期号:40 (4): 78-90 被引量:3
标识
DOI:10.2478/msp-2022-0046
摘要

Abstract Aerosol jet printing is a contactless direct-write technique that could be used for the deposition of a variety of materials. First, used for electric paths, the technology was explored for many applications. The substantial part of the process is the generation of aerosols. The size of the droplets and the stability of the process affect the quality of the sprayed lines. This article investigates the diameter of the sprayed droplets, allowing future comparison of the results with sprayed lines. Droplets from ultrasonic and pneumatic generators were sprayed at their outlet on the polyethylene terephthalate (PET) foil. Using a digital microscope and the built-in algorithm, the diameter of the droplets was measured, and the dataset was collected as CSV files and served as a background to the box plot. Scanning electron microscopy (SEM) and atomic force microscopy (AFM) scans were applied to verify the results obtained. The ink parameters used in the process have an influence on the aerosol generation and droplet diameter, whereas the carrier gas pressure has an impact mostly on the droplet diameter. In this case, the aerosol was produced from three types of ink in combination with two generators. For inks with a dynamic viscosity below 6.5 m·Pa −1 ·s −1 a stable range of 5–10 μm droplet diameter was observed. A high-viscosity ink (7.5–10.5 m·Pa −1 ·s −1 ) produced droplets with diameter in the range of 6–25 μm. The diameter of the droplet decreased from 7–22 μm to 1–5 μm with a reduction in the dynamic viscosity from 7.5–10.5 m·Pa −1 ·s −1 to 4.5–5.5 m·Pa −1 ·s −1 .
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