Effect of silane coupling agent on compatibility interface and properties of wheat straw/polylactic acid composites

材料科学 复合材料 热重分析 聚乳酸 复合数 硅烷 极限抗拉强度 动态力学分析 热稳定性 扫描电子显微镜 傅里叶变换红外光谱 结晶度 聚合物 化学工程 工程类
作者
Kang Chen,Ping Li,Xingong Li,Chenggang Liao,Xianjun Li,Yingfeng Zuo
出处
期刊:International Journal of Biological Macromolecules [Elsevier BV]
卷期号:182: 2108-2116 被引量:82
标识
DOI:10.1016/j.ijbiomac.2021.05.207
摘要

To improve the performance of wheat straw/polylactic acid (WS/PLA) composites, four different silane coupling agents were used for constructing compatible interfaces and then examined by scanning electron microscopy, Fourier transform-infrared spectroscopy, X-ray diffractometry and thermogravimetric analysis. The blending and tensile strengths of silane-modified composites were effectively enhanced, with KH-570-modified composite exhibiting the best blending and tensile strengths. Water resistance analysis of silane-modified composites was reduced and contact angles larger, indicating that water resistance performance of this composite had been effectively improved. The KH-570-modified composite exhibited the best water resistance performance. Strain scanning showed that, in the linear viscoelastic region, the storage modulus (G') of modified composite was larger than that of unmodified composites. Frequency scanning showed that the G' and complex viscosity (η*) of modified composites were greater than those of unmodified composites. From strain analysis and frequency scanning, the modified performance of the silane agent was observed to effectively improve composite interfacial compatibility, with KH-570-modified composite exhibiting the best effect. XRD analysis showed that silane coupling agent modification improved the crystallinity of composites with the improvement of KH-570 the best. And the thermal stability of silane-modified composites was improved and the thermal stability of KH-570-modified composite the best.
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