电化学发光
纳米棒
草甘膦
纳米技术
材料科学
银纳米粒子
纳米颗粒
环境科学
化学
检出限
色谱法
生态学
生物
作者
Daniel Canseco-Caballero,Antonio Ledezma‐Pérez,Carmen Alvarado‐Canché,M. Castillo,Carlos Gallardo‐Vega,Enrique Díaz Barriga‐Castro,Agustín L. Herrera‐May,Esmeralda Saucedo‐Salazar,Arxel de León
标识
DOI:10.1016/j.optmat.2023.114101
摘要
Glyphosate (GlyP) is a worldwide commonly used herbicide. However, it has an undesirable impact on the ecosystem threatening human health. Therefore, a quick, easy, and reliable way to identify and quantify its presence in food samples is currently required. Electrochemiluminescence (ECL) sensors are outstanding systems for achieving this important goal. Here, we report a wet approach for hydrothermal synthesis of ZnO nanorods functionalized with silver nanoparticles (ZnO/AgNp). Incorporating this hybrid material into ruthenium-based ECL sensors enables the construction of a reliable sensor that exhibits an ECL signal enhancement with exceptional stability for the analytical quantification of GlyP. Our straightforward method allowed us to develop a calibration curve over the GlyP range of 25–200 ppm and test walnut samples obtained on the local farm. The study confirms the possible translocation of Glyp to nuts and husks.
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