Study of the microstructure and mechanical performance of C-X stainless steel processed by selective laser melting (SLM)

材料科学 微观结构 选择性激光熔化 马氏体 奥氏体 选区衍射 沉淀硬化 扫描电子显微镜 高分辨率透射电子显微镜 极限抗拉强度 透射电子显微镜 压痕硬度 冶金 降水 奥氏体不锈钢 能量色散X射线光谱学 复合材料 纳米技术 腐蚀 物理 气象学
作者
Xingchen Yan,Chaoyue Chen,Cheng Chang,Dongdong Dong,Ruixin Zhao,Richard Jenkins,Jiang Wang,Zhongming Ren,Min Liu,Hanlin Liao,Rocco Lupoi,Shuo Yin
出处
期刊:Materials Science and Engineering A-structural Materials Properties Microstructure and Processing [Elsevier BV]
卷期号:781: 139227-139227 被引量:84
标识
DOI:10.1016/j.msea.2020.139227
摘要

In this study, a new precipitation hardening stainless steel (PHSS), C-X stainless steel, was manufactured using selective laser melting (SLM) technology. Following SLM fabrication, a series of heat treatments were applied to improve the mechanical properties of the as-built samples. The microstructure precipitates distribution and evolution, and mechanical properties of SLM C-X stainless steels in the as-built and heat-treated conditions were systematically studied using scanning electron microscope (SEM), X-ray diffraction (XRD), and transmission electron microscope (TEM). The XRD spectrum revealed that solution treatment resulted in the formation of a complete martensite phase, and a reverted austenite (γ') phase formed after aging treatment. The TEM analysis indicated that numerous dislocations and nanoprecipitates were dispersed within the martensite matrix for both the as-built and aged samples. The rod-like NiAl precipitates with a size range of 3–25 nm for the as-built samples and 7–30 nm for the solution-aged samples were determined through high-resolution TEM (HRTEM), selected area electron diffraction (SAED), and energy-dispersive X-ray spectroscopy (EDS). Furthermore, the microhardness of the SLM C-X stainless steel parts was found to significantly improve from 350 HV0.2 in the as-built state to 510 HV0.2 in the solution-aged state. The ultimate tensile strength (UTS) of the SLM C-X stainless steel parts also increased from 1043 MPa in the as-built state to 1601 MPa after solution-aging heat treatment.
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