苯肼
化学
氨基脲
查尔酮
盐酸盐
吡唑啉
醋酸
酰肼
核化学
质子核磁共振
产量(工程)
氨基脲
碳-13核磁共振
有机化学
材料科学
冶金
作者
M. Emayavaramban,N. Santhi,C. Gopi,C. Manivannan,A. Raguraman
出处
期刊:International Letters of Chemistry, Physics and Astronomy
[SciPress Ltd.]
日期:2013-09-01
卷期号:14: 172-185
被引量:17
标识
DOI:10.18052/www.scipress.com/ilcpa.14.172
摘要
A chalcone was prepared by the reaction of 4-methylbenzaldehyde with 4-methylacetophenone in dilute methanolic sodium hydroxide solution under ultrasonic irradiationin the water bath of an ultrasonic cleaner at room temperature. Treatment of this chalcone with thiosemicarbazide/semicarbazide hydrochloride/benzhydrazide/benzenesulphonyl hydrazide/phenylhydrazine hydrochloride afforded the corresponding 2-pyrazoline in good yields. All the new compounds have been characterized by IR, 1 H-NMR, 13 CNMR spectral data. All the target compounds were evaluated for their In Vivo anti-diabetic activity in rates in comparison with as reference drug.
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