Asymmetric SO3CF3−‐Grafted Boron‐Center Anion Enables Boron‐Containing Interphase for High‐Performance Rechargeable Mg Batteries

Advanced Functional MaterialsEarly View 2314146 Research Article Asymmetric SO3CF3−-Grafted Boron-Center Anion Enables Boron-Containing Interphase for High-Performance Rechargeable Mg Batteries Xueting Huang, Xueting Huang College of Materials Science and Engineering, Chongqing University, Chongqing, 400044 P. R. China National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this authorShuangshuang Tan, Corresponding Author Shuangshuang Tan [email protected] College of Materials Science and Engineering, Chongqing University, Chongqing, 400044 P. R. China National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. China E-mail: [email protected]; [email protected]; [email protected]Search for more papers by this authorJinlong Chen, Jinlong Chen National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. China College of Chemical Engineering, Sichuan University of Science and Engineering, Zigong, Sichuan, 643000 P. R. ChinaSearch for more papers by this authorZiwei Que, Ziwei Que National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. China School of Chemistry and Chemical Engineering, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this authorRongrui Deng, Rongrui Deng College of Materials Science and Engineering, Chongqing University, Chongqing, 400044 P. R. China National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this authorJuncai Long, Juncai Long State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan, 430070 P. R. ChinaSearch for more papers by this authorFangyu Xiong, Fangyu Xiong College of Materials Science and Engineering, Chongqing University, Chongqing, 400044 P. R. China National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this authorGuangsheng Huang, Guangsheng Huang College of Materials Science and Engineering, Chongqing University, Chongqing, 400044 P. R. China National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this authorXiaoyuan Zhou, Xiaoyuan Zhou National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this authorLingjie Li, Corresponding Author Lingjie Li [email protected] National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. China School of Chemistry and Chemical Engineering, Chongqing University, Chongqing, 400044 P. R. China E-mail: [email protected]; [email protected]; [email protected]Search for more papers by this authorJingfeng Wang, Jingfeng Wang College of Materials Science and Engineering, Chongqing University, Chongqing, 400044 P. R. China National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this authorLiqiang Mai, Corresponding Author Liqiang Mai [email protected] orcid.org/0000-0003-4259-7725 State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan, 430070 P. R. China E-mail: [email protected]; [email protected]; [email protected]Search for more papers by this authorFusheng Pan, Fusheng Pan College of Materials Science and Engineering, Chongqing University, Chongqing, 400044 P. R. China National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this author Xueting Huang, Xueting Huang College of Materials Science and Engineering, Chongqing University, Chongqing, 400044 P. R. China National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this authorShuangshuang Tan, Corresponding Author Shuangshuang Tan [email protected] College of Materials Science and Engineering, Chongqing University, Chongqing, 400044 P. R. China National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. China E-mail: [email protected]; [email protected]; [email protected]Search for more papers by this authorJinlong Chen, Jinlong Chen National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. China College of Chemical Engineering, Sichuan University of Science and Engineering, Zigong, Sichuan, 643000 P. R. ChinaSearch for more papers by this authorZiwei Que, Ziwei Que National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. China School of Chemistry and Chemical Engineering, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this authorRongrui Deng, Rongrui Deng College of Materials Science and Engineering, Chongqing University, Chongqing, 400044 P. R. China National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this authorJuncai Long, Juncai Long State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan, 430070 P. R. ChinaSearch for more papers by this authorFangyu Xiong, Fangyu Xiong College of Materials Science and Engineering, Chongqing University, Chongqing, 400044 P. R. China National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this authorGuangsheng Huang, Guangsheng Huang College of Materials Science and Engineering, Chongqing University, Chongqing, 400044 P. R. China National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this authorXiaoyuan Zhou, Xiaoyuan Zhou National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this authorLingjie Li, Corresponding Author Lingjie Li [email protected] National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. China School of Chemistry and Chemical Engineering, Chongqing University, Chongqing, 400044 P. R. China E-mail: [email protected]; [email protected]; [email protected]Search for more papers by this authorJingfeng Wang, Jingfeng Wang College of Materials Science and Engineering, Chongqing University, Chongqing, 400044 P. R. China National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this authorLiqiang Mai, Corresponding Author Liqiang Mai [email protected] orcid.org/0000-0003-4259-7725 State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan, 430070 P. R. China E-mail: [email protected]; [email protected]; [email protected]Search for more papers by this authorFusheng Pan, Fusheng Pan College of Materials Science and Engineering, Chongqing University, Chongqing, 400044 P. R. China National Engineering Research Center for Magnesium Alloys, Chongqing University, Chongqing, 400044 P. R. ChinaSearch for more papers by this author First published: 04 January 2024 https://doi.org/10.1002/adfm.202314146Read the full textAboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onEmailFacebookTwitterLinkedInRedditWechat Abstract Mg(SO3CF3)2 (Mg(OTf)2) is a simple and cost-effective magnesium salt, which can promote the future applications of rechargeable magnesium batteries (RMBs). However, the simple Mg(OTf)2/ether electrolytes suffer from poor electrochemical properties due to the low solubility of Mg(OTf)2 and the serious decomposition passivation of the [Mg2+-OTf−] ion pair on Mg. Herein, the OTf− anion is successfully grafted on low-cost fluoride boronic esters (B(OCxHyF2x-y+1)3) to obtain the asymmetric and weak-coordination boron-center [B(OCxHyF2x-y+1)3OTf]− anion in ether electrolytes. The -OCH2CF3 (TFE) groups in B(TFE)3 effectively realize the charge delocalization of the OTf− and B-O plane, restraining the independent decomposition of the [Mg2+-OTf−] ion pair. The co-decomposition of the asymmetric [B(TFE)3OTf]− induces the formation of the B-containing organic/inorganic interphase, thus achieving a reversible Mg plating/stripping. After the further solubilization reaction, the obtained electrolyte exhibits a high average coulombic efficiency of 98.13% and long-term cycling stability (1000 h). Notably, the long cycling life (capacity retention of 90.2% after 600 cycles at 1 C) and high-rate capacity (43.0 mAh g−1 at 5 C) of the Mg/Mo6S8 full cell demonstrate a favorable electrolyte/cathode compatibility. This work brings new insights to design the new-type and low-cost Mg-salts and high-performance electrolytes for commercial RMBs. Conflict of Interest The authors declare no conflict of interest. Open Research Data Availability Statement The data that support the findings of this study are available from the corresponding author upon reasonable request. Supporting Information Filename Description adfm202314146-sup-0001-SuppMat.pdf21.1 MB Supporting Information Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article. References 1M. Mao, T. Gao, S. Hou, C. Wang, Chem. Soc. 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