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The effect of different parameters on the wear, surface properties, and shear bond strength of monolithic zirconia CAD/CAM restorative materials

材料科学 立方氧化锆 复合材料 复合数 粘结强度 抗剪强度(土壤) 陶瓷 胶粘剂 图层(电子) 环境科学 土壤科学 土壤水分
作者
Seval BAŞPINAR ALPER,Neslihan Tekçe,Elif Sevilay Yıldırım,Elif İlgi Sancak,Sinan Fi̇dan
出处
期刊:Journal of Adhesion Science and Technology [Taylor & Francis]
卷期号:37 (23): 3379-3392
标识
DOI:10.1080/01694243.2023.2194069
摘要

To investigate the effects of preparation order and sandblasting procedures (different particle sizes and sandblasting times) on the wear, surface properties, and shear bond strength of zirconia material. A total of 130 test specimens were fabricated from Katana-Zirconia (n = 10). 70 test samples were sintered. Control, pre-sintered, and sintered groups were formed. The initial weights of the samples were measured. Sandblasting treatments were performed from a distance of 10-mm at 2-bar pressure for 10, 15, and 20-s with 29-µm and 50-µm Al2O3. The weight measurement was repeated. Subsequently, pre-sintered groups were sintered. Samples were scanned using a Nanovea-PS50. Ra, Rz, and Sa values ​​were recorded. Then, samples were embedded in acrylic. Composite bars were fabricated using a Teflon mold and bonded to the samples with G-CEM Link-Force. The shear bond strength test was performed. The data were analyzed using the Shapiro-Wilk test and two-way analysis ANOVA (p < 0.05). The highest Ra values were 1.198 ± 0.105 (Group-6) for PSZ and 0.267 ± 0.015 (Group-6) for SZ. Sa data demonstrated the highest values of 4.628 ± 1.541 (Group-6) for PSZ. The highest SBS values were 15.35 ± 2.75 (Group-4) for PSZ and 12.76 ± 2.39 (Group-1) for SZ. PSZ showed higher wear amount, Ra, Rz, Sa, and SBS in Groups 4 and 5 (p < 0.05). Pre-sintered and sintered zirconia showed different dependencies on sandblasting parameters regarding weight loss, Ra, Rz, Sa, and SBS. Sandblasting zirconia materials with 50-µm Al2O3 for 10 or 15-s before sintering may have beneficial effects on surface roughness and SBS.
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