二氧化硫
响应面法
硫黄
纳米颗粒
材料科学
线性范围
二氧化硅
灵敏度(控制系统)
分析化学(期刊)
检出限
化学工程
纳米技术
化学
无机化学
色谱法
复合材料
电子工程
冶金
工程类
作者
Fuxiu Yang,Wenjuan Zhang,Youxi Zhao,Yizhi Ji,Baining Liu,Kaowen Zhou
标识
DOI:10.1002/slct.202001415
摘要
Abstract In the past, the working conditions of cataluminescence (CTL) method were simply determined by single factor experiment. This paper will illustrate the optimization of working conditions of a novel sulfur dioxide gas sensor based on Au/CoO‐2La 2 WO 6 nanoparticles by response surface methodology (RSM). Under optimized working conditions, analytical wavelength 522.77 nm, reaction temperature 111.15 °C and carrier gas velocity 144.92 ml/min, the sensitivity of the method can be increased by 6.4 %. The optimization process is universal for many multi parameter processes. There is a good linear relationship between the CTL intensity and the concentration of sulfur dioxide in the range of 0.06–120 mg/m 3 with a detection limit (3σ) of 0.015 mg/m 3 . The sensing properties of sensitive material were investigated. The results indicated that nano‐Au/CoO‐2La 2 WO 6 could be a good candidate for fabricating sulfur dioxide gas sensors.
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