溶胶凝胶
聚酰亚胺
材料科学
复合数
热稳定性
扫描电子显微镜
纳米-
傅里叶变换红外光谱
化学工程
聚酰胺
纳米尺度
复合材料
纳米技术
图层(电子)
工程类
作者
Hao Zhou,X.G. Liu,Defang Zhao,Fuchang Lin,Yong Fan
出处
期刊:Pigment & Resin Technology
[Emerald (MCB UP)]
日期:2008-05-23
卷期号:37 (3): 161-166
被引量:3
标识
DOI:10.1108/03699420810871002
摘要
Purpose The purpose of this paper is to synthesise and characterise nano‐alumina hybrid polyimide (PI) films. Design/methodology/approach PI nano‐composite films containing definitive contents of Al 2 O 3 were prepared by the sol‐gel process of aluminum isopropoxide in the N, N′‐dimethylacetamide solution of polyamide acid. The films were characterised by Fourier transform infrared spectroscope, atomic forced microscope, and X‐ray fluorescent spectroscope (XRF). The thermal stability of the composite films was tested by TG. Findings PI nano‐Al 2 O 3 films were prepared by the sol‐gel method. The XRF is an effective way to detect the inorganic phase of the composite films and measure the content of nano‐Al 2 O 3 . Research limitations/implications There are seldom reports about the PI composites containing Al 2 O 3 through sol‐gel process. Practical implications PI has been widely used in the fields of aviation micro‐electron and less costly dyes. Originality/value Improved electricity insulation property of the PI films. Al 2 O 3 particles were distributed homogeneously in the PI in nano‐scale by means of sol‐gel process.
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