Microstructure Evolution in Mg<sub>98.6</sub>Y<sub>1</sub>Zn<sub>0.4</sub> Alloys and the Development by Hot Deformation Examined by Synchrotron Radiation Small- and Wide-Angle Scattering

Synchrotron radiation small- and wide-angle scattering measurements have been performed for Mg98.6–Y1–Zn0.4 alloys. In the early stage of phase transformation from supersaturated solid solutions, isotropic scattering suggesting segregation at grain boundaries was observed. It grew with temperature during heating the sample at a constant rate of 0.133 K/s. Above 600 K where introduction of stacking faults is expected, needle-like scattering became visible, which represents platelet shape segregation of cluster layers called cluster arranged layer (CAL). The layer eventually developed to form multiple layers, cluster arranged nano plates (CANaP) at higher temperatures. Microstructure change by hot rolling after the heat treatments has been examined from a viewpoint of kink-deformed microstructures.