介质阻挡放电
电介质
纳米-
胶体
等离子体
化学工程
纳米银
粒子(生态学)
催化作用
溶剂
粒径
分析化学(期刊)
纳米技术
材料科学
物理
化学
色谱法
有机化学
光电子学
地质学
工程类
海洋学
量子力学
作者
Zahra Bahrami,Mohammad Reza Khani,Babak Shokri
摘要
In this study, cylindrical dielectric barrier discharge plasma was used to study the catalytic effect on chemical methods of silver nano-particles for the first time. In this method, the processing time is short and the temperature of reaction is low. Also, the reactor is very simple, inexpensive, and accessible. In this work, pure AgNO3 as the precursor agent and poly vinyl pyrrolidone as the macromolecular surfactant were dissolved in ethanol as the solvent. UV-Vis and XRD were used to identify the colloidal and powder nano-particles, respectively. Optical emission spectroscopy was also used to identify the active species in plasma. Effects of gas flow rate, voltage, volume of solution, and processing time were also studied. Moreover, TEM and SEM images presented the mean diameter of nano-particle size around 10 to 20 nm. The results have been very promising.
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