Infiltration of silica slurry into silica-based ceramic cores prepared by selective laser sintering based on pre-sintering

材料科学 烧结 抗弯强度 泥浆 陶瓷 多孔性 方石英 复合材料 模具 选择性激光烧结 石英
作者
Jie Zhang,Jia‐Min Wu,Heng Liu,Y.B. Zhang,Chun-Sheng Ye,Yusheng Shi
出处
期刊:Ceramics International [Elsevier BV]
卷期号:49 (19): 31477-31484 被引量:9
标识
DOI:10.1016/j.ceramint.2023.07.095
摘要

The silica-based ceramic core is an important mold for manufacturing hollow blades. The preparation of silica-based ceramic cores by combining selective laser sintering (SLS) and vacuum infiltration (VI) technologies is a promising approach. To enhance infiltration effect, pre-sintering was introduced to obtain the bodies with high porosity and hydrophilicity. The infiltrated silica content increased from 29.58 wt% for samples infiltrated once to 68.91 wt% for samples infiltrated three times. The increase of silica content in the matrix reduced the porosity of final ceramics, thus improving the room-temperature flexural strength. The infiltrated silica gradually transformed into cristobalite during the high-temperature test, which improved the high-temperature flexural strength and creep resistance. When the final-sintering temperature was 1225 °C, room-temperature and high-temperature flexural strength reached 21.17 MPa and 21.21 MPa, respectively, due to the enhanced sintering necks and low porosity. These results indicate that our work provides a promising route to fabricate silica-based ceramic cores by SLS technology.
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