材料科学
光催化
纳米复合材料
微晶
复合数
降级(电信)
粒径
复合材料
带隙
壳聚糖
化学工程
光电子学
冶金
电子工程
催化作用
工程类
化学
生物化学
作者
Saba Afzal,Nurhidayatullaili Muhd Julkapli,Kian Mun Lee
标识
DOI:10.1016/j.mssp.2021.105891
摘要
Conventional methods for the nitrophenols (NP) treatment only transform the contaminant from one phase to another and require long incubation time. Therefore, in this paper, highly active TiO2/chitosan/Fe3O4 nanocomposites were synthesized and optimized by varying TiO2, chitosan (CS), and Fe3O4 loading. Each individual component exhibits a strong influence on particle size, magnetic and optical properties of the resultant composite. The optimum loading was achieved in TCF2 composite which displays a remarkable improvement in charge carrier separation and bandgap narrowing (2.85 eV) than all other composites. The improved optical properties of TCF2 are due to its larger crystallite size (24.5 nm) than other composites, as crystallite size is inversely related to the bandgap of the sample. The optimum photocatalytic activities were observed for TCF2 with >90% degradation for 180 min of under solar light exposure. Thus, the photocatalyst system has an advantage on easy recoverability potential to be a new appealing technology for NP treatment.
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