X射线光电子能谱
纳米晶材料
扫描电子显微镜
材料科学
薄膜
透射电子显微镜
拉曼光谱
椭圆偏振法
化学工程
阳极
分析化学(期刊)
化学
纳米技术
光学
复合材料
色谱法
电极
物理化学
工程类
物理
作者
Yefeng Yang,Xiaoqing Du,Yang Yang,Li Jun Jiang,Zhao Zhang,Jianqing Zhang
出处
期刊:Journal of The Electrochemical Society
[The Electrochemical Society]
日期:2015-01-01
卷期号:162 (4): D166-D173
被引量:9
摘要
Nanocrystalline ceria thin films of yellowish color have been photo-assisted anodic deposited in the electroplating solution containing various volume ratio of ethanol (0, 10, 40, 70 and 100%) onto 316 L surface, and the influence of ethanol content on the formation of ceria films were studied with scanning electron microscopy, ellipsometry, X-ray diffraction, transmission electron microscopy, Raman and X-ray photoelectron spectroscopy. Results show that both the film thickness and particle size of ceria layers increase whereas both the film porosity and Ce(III) content decrease with the augment of ethanol content from 0 to 70%; The important role of ethanol content in enhancing the anodic deposition rate of ceria film may be mostly achieved by the simultaneously photo generated electrons (e−cb).
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