东莨菪碱
葡聚糖
色谱法
硅胶
化学
柱色谱法
高效液相色谱法
凤仙花
有机化学
植物
生物
医学
病理
酶
栽培
替代医学
作者
Jianchao Zhang,Wen‐Jun He,Liu Yan-wen,Ning‐Hua Tan
出处
期刊:China journal of Chinese materia medica
[China Journal of Chinese Materia Medica]
日期:2016-01-01
被引量:2
标识
DOI:10.4268/cjcmm20160116
摘要
Eight compounds were isolated from the 50% ethanol extract of Impatiens pritzllii var.hupehensis through various column chromatography methods including silica gel, Sephadex LH-20, and preparative HPLC. Their structures were elucidated as 2,6-dimethyl-2-vinyl-2,3,4,7-tetrahydrooxepine(1), 1,3,6-trihydroxy-7-methyl-anthraquinone(2),4-hydroxybenzaldehyde(3),4-(3-methoxy-4-hydroxyphenyl)-2-butanone(4), podophyllotoxin(5),scopoletin(6), α-spinasterol(7) and 3-O-β-D-glucopyranosyl-α-spinasterol(8) based on the NMR and MS spectral data. Compound 1 is new compound and compounds 2-8 are isolated from this plant for the first time.
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