热重分析
硫黄
碳纤维
材料科学
X射线光电子能谱
柠檬酸
拉曼光谱
扫描电子显微镜
解吸
无机化学
化学工程
吸附
核化学
化学
复合数
有机化学
复合材料
工程类
物理
光学
冶金
作者
Liping Zhao,Lihe Zhao,Ye Zhao,Bangyi Zhang,Gang Liu,Peng Zhang
标识
DOI:10.1016/j.aej.2021.10.053
摘要
A nitrogen-sulfur dual-doped citric-acid porous carbon/sulfur (NS-CAPC/S) materials was prepared by an easy hydrothermal method applying glutathione as nitrogen-sulfur origin and citric-acid carbon as carbon origin. The detailed structure of the materials was determined through raman spectroscopy, X-ray photoelectron spectroscopy, and X-ray diffraction tests. The appearance of the materials was investigated via transmission electron microscopy and scanning electron microscopy methods. N2 adsorption–desorption isotherm was applied to test its pore size distribution and pore structure. Thermogravimetric analysis (TGA) was utilized to identify the mass ratio of sulfur. The NS-CAPC/S materials was employed as positive electrode material in Li-S batteries. Electrochemical performance revealed the prepared NS-CAPC/S composite possessed good specific capacity, exceptionally high cycle stability and excellent rate performance.
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