煅烧
X射线光电子能谱
高分辨率透射电子显微镜
兴奋剂
锐钛矿
材料科学
金红石
离子
分析化学(期刊)
透射电子显微镜
锌
无机化学
化学
纳米技术
化学工程
光催化
冶金
催化作用
工程类
生物化学
有机化学
光电子学
色谱法
作者
Yanlong Yu,Jingsheng Wang,Wei Li,Wenjun Zheng,Yaan Cao
出处
期刊:CrystEngComm
[The Royal Society of Chemistry]
日期:2015-01-01
卷期号:17 (27): 5074-5080
被引量:53
摘要
A series of Zn doped TiO2 is prepared via a sol–gel method by changing the concentration of Zn ions and calcination temperature. To investigate the existing states of introduced Zn, the transformation of existing states and the phase transition for the Zn doped TiO2 samples, high resolution transmission electron microscopy (HRTEM), X-ray photoelectron spectroscopy (XPS) and X-ray diffraction (XRD) techniques are applied. The existing states of Zn2+ ions and the transformation of existing states (O–Zn–Cl and ZnTiO3) in Zn doped TiO2 are closely related to the calcination temperature and concentration of introduced Zn ions, as well as the phase transition temperature from anatase to rutile. This work can be helpful for a better realization about the doping mechanism of Zn2+ ions in Zn doped TiO2.
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