连续搅拌釜式反应器
光催化
材料科学
工艺工程
苯硼酸
化学工程
反应性(心理学)
化学
催化作用
有机化学
工程类
医学
替代医学
病理
作者
Rizvi Syed Aal E Ali,Jiaolong Meng,Xuefeng Jiang
标识
DOI:10.1021/acs.oprd.3c00328
摘要
Photocatalysis has been comprehensively applied to diverse valuable chemical transformations. However, photocatalytic processes have encountered obstacles in gaining wide acceptance in industry, primarily due to scale-up challenges, especially in heterogeneous systems involving equivalent amounts of solids. We designed a photo-continuous stirred tank reactor (CSTR) protocol for heterogeneous photocatalytic processes, which is capable of multiphasic processes with excellent adaptability. Furthermore, glass-wool-supported photocatalyst was successfully made, applied, and recycled at least 12 times without any decrease in hydroxylation of phenylboronic acid in reactivity, enabling gram scale synthesis with high efficiency in photo-CSTR.
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