二硫化钨
钨
纳米片
材料科学
纳米材料
高分辨率透射电子显微镜
纳米技术
化学工程
X射线光电子能谱
热液循环
水热合成
二硫化钼
溴化物
无机化学
透射电子显微镜
冶金
化学
工程类
作者
Deqing Zhang,Tingting Liu,Junye Cheng,Shuang Liang,Jixing Chai,Xiuying Yang,Hao Wang,Guangping Zheng,Maosheng Cao
标识
DOI:10.1016/j.ceramint.2019.03.177
摘要
The hydrothermal method was utilized to synthesize flat sheet-like tungsten disulfide with a single-crystal structure, using sodium diethyldithiocarbamate, tungsten hexachloride and cetyltrimethylammonium bromide as a reducing agent and a sulfur source, a tungsten source and a surfactant, respectively. The controllable synthesis of the tungsten disulfide nanosheet was realized by controlling the types of surfactants, which was characterized by XRD, FTIR, XPS, SEM, TEM, HRTEM, BET, UV-vis and PL. Due to the unique flat sheet morphology and unique electronic characteristic of the synthesized tungsten disulfide nanosheets, they could be promising nanomaterials for electronic devices.
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