原位
透射电子显微镜
电子显微镜
扫描透射电子显微镜
扫描共焦电子显微镜
高分辨率透射电子显微镜
材料科学
显微镜
能量过滤透射电子显微镜
分辨率(逻辑)
光学
分析化学(期刊)
纳米技术
化学
物理
计算机科学
人工智能
有机化学
色谱法
作者
Pratibha L. Gai,Edward Boyes
摘要
Abstract Advances in atomic resolution in situ environmental transmission electron microscopy for direct probing of gas‐solid reactions, including at very high temperatures (∼2000°C) are described. In addition, recent developments of dynamic real time in situ studies at the Angstrom level using a hot stage in an aberration corrected environment are presented. In situ data from Pt/Pd nanoparticles on carbon with the corresponding FFT/optical diffractogram illustrate an achieved resolution of 0.11 nm at 500°C and higher in a double aberration corrected TEM/STEM instrument employing a wider gap objective pole piece. The new results open up opportunities for dynamic studies of materials in an aberration corrected environment. Microsc. Res. Tech., 2009. © 2009 Wiley‐Liss, Inc.
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