单斜晶系
氯化物
化学
立体化学
一锅法合成
药物化学
晶体结构
有机化学
催化作用
作者
Daniel F. Brayton,Karen I. Goldberg,Werner Kaminsky,D. Michael Heinekey
标识
DOI：10.1080/10426500801967781
摘要
A convenient one-pot synthesis of (t-Bu)2P(O)Cl (1) from m-chloroperbenzoic acid and (t-Bu)2PCl is described. The byproduct m-chlorobenzoic acid is neutralized by addition of Et3N. Complex 1 crystallizes in the monoclinic space group P21/c (No. 14), with a = 5.9637(2) Å, b = 11.4734(4) Å, c = 16.2400(5) Å and β = 107.7160(14).
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