硼
微观结构
材料科学
烧结
无定形固体
热离子发射
场电子发射
粒度
陶瓷
化学工程
氧化硼
制作
纳米技术
冶金
分析化学(期刊)
结晶学
化学
氧化物
电子
有机化学
医学
物理
替代医学
病理
量子力学
工程类
作者
Lihong Bao,J.X. Zhang,Shen‐Lin Zhou,Yongfeng Wei,Zhihe Dou
出处
期刊:Physica status solidi
日期:2011-09-02
卷期号:9 (1): 11-14
被引量:8
标识
DOI:10.1002/pssc.201084151
摘要
Abstract Two different structured boron sources have been used for the fabrication of LaB 6 ceramics and their effects on the sintering temperature, microstructure and emission properties were investigated. The results show that the reaction temperature of amorphous boron and La to form LaB 6 is 1200 °C, which is 150 °C lower than the reaction using crystalline boron. The grain size of LaB 6 prepared by amorphous boron and La is 150 nm, which is much smaller than that of crystalline boron ∼2 μm at the same sintering condition. With the grain size decreasing from 5 μm to 150 nm, the LaB 6 thermionic emission current density increases significantly and the field emission turn‐on field decreases from 1500 V to 1300 V. Using amorphous boron nanopowder can not only enhance the microstructure but also improve the emission properties. (© 2012 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)
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