聚偏氟乙烯
膜
石墨烯
材料科学
傅里叶变换红外光谱
罗丹明B
化学工程
X射线光电子能谱
纳米片
衍射仪
结晶紫
甲基橙
甲基蓝
复合材料
纳米技术
化学
扫描电子显微镜
有机化学
聚合物
医学
生物化学
催化作用
病理
光催化
工程类
作者
Xiaojin Wei,Xiaotao Fan,Yimeng Deng,Liqiang Li,Xiaolong Han,Ping Lu,Chao Hua
标识
DOI:10.1016/j.jiec.2022.04.024
摘要
The hydrothermal reduced graphene (rGO) and the layered MoS2 nanosheets prepared by the liquid-phase stripping method were blended, and then the MoS2-rGO composite membranes were prepared on the polyvinylidene fluoride (PVDF) supporting membranes by vacuum filtration method. A variety of characterization methods such as Fourier transform infrared spectrometer (FT-IR), X-ray photoelectron spectroscopy (XPS) and X-ray diffractometer (XRD) were used to verify the successful introduction of MoS2 into rGO layers and the changes of interlayer structure of the MoS2-rGO membranes. Finally, the effect of MoS2 loading on separation performance of the MoS2-rGO composite membrane was investigated. The results show that the separation performance of the membrane with 33.33% of MoS2 loading (M−rG−3) is the most excellent. The permeability of M−rG−3 membrane is 118.21 L m-2h−1 bar−1, which is about 4.4 times that of the pristine rGO membrane. Meanwhile, the rejection of the M−rG−3 membrane for Methyl blue, Crystal violet, Rhodamine B, and Congo red all exceed 80%.
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