沸石
结晶度
埃洛石
煅烧
结晶
化学工程
材料科学
热稳定性
吸附
水热合成
热液循环
催化作用
化学
有机化学
复合材料
工程类
作者
Xinmei Lu,Liying Liu,Haoran Liu,Tian Guo,Peng Gao,Zhuo Li,Zhe Wang
标识
DOI:10.1016/j.jtice.2022.104281
摘要
: Zeolite-X has good selective adsorption, ion exchange and hydrophilic properties, and has been widely studied and applied in the chemical industry. Halloysite nanotubes (HNTs), with a unique tubular microstructure, natural availability, and low cost. The use of HNTs to synthesize X zeolites reduces production costs, leading to large-scale industrial production applications. : In this study, zeolite-X, with high crystallinity and a large specific surface area, was synthesized, for the first time, by purifying HNTs, calcining HNTs and hydrothermal synthesis. The influence of calcination time, crystallization temperature, crystallization time and NaOH concentration on the crystal phase and the static saturated water absorption of zeolite-X were investigated. The structure, shape and thermal stability of the synthesized zeolite-X were characterized by XRD, TEM, and FT-IR techniques and analysis methods. : Zeolite-X synthesized by this method has good crystallinity, uniform particle size and similar thermal stability to industrial zeolite. This study reports a new synthesis method to obtain zeolite 13X, with potential application in CO2 capture from flue gases.
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