Precisely Controlled Reproducible Synthesis of Palladium Nanoparticles inside Metal-Organic Frameworks with H2 Gas as Reductant: Effects of Framework Crystallinity and H2 Gas Pressure

Herein, we succeeded in reproducibly synthesizing palladium nanoparticles with narrow size distribution inside metal–organic frameworks (MOFs) by using pressured H2 gas as a reductant. In addition, by controlling the crystallinity of the MOFs, the particle size could be precisely controlled. Herein, we succeeded in reproducibly synthesizing palladium nanoparticles with narrow size distribution inside metal–organic frameworks (MOFs) by using pressured H2 gas as a reductant. In addition, by controlling the crystallinity of the MOFs, the particle size could be precisely controlled.