Surficial Reconstruction of Pt–Ni/NiS and Its Effect on Electrocatalytic Hydrogen Evolution in Alkaline Medium

Cyclic voltammetry pretreatment of Pt-based electrocatalysts has been proven to be a normal activation process on achieving the optimal alkaline hydrogen evolution performance. Until now, the congruent relationship between the microstructural evolution and performance improvement during this process has rarely been reported. Herein, when the