银纳米粒子
傅里叶变换红外光谱
核化学
Zeta电位
动态光散射
透射电子显微镜
光谱学
化学
水溶液
纳米颗粒
催化作用
吸光度
选区衍射
材料科学
分析化学(期刊)
纳米技术
化学工程
色谱法
有机化学
物理
量子力学
工程类
作者
Thomas Nesakumar Jebakumar Immanuel Edison,Yong Rok Lee,Mathur Gopalakrishnan Sethuraman
标识
DOI:10.1016/j.saa.2016.02.044
摘要
Facile green synthesis of silver nanoparticles (AgNPs) using aqueous bark extract of Terminalia cuneata has been reported in this article. The effects of concentration of the extract, reaction time and pH were studied by UV–Vis spectroscopy. Appearance of yellow color with λmax around ~ 420 nm suggested the formation of AgNPs. The stable AgNPs were further characterized by Fourier transform infrared (FT-IR) spectroscopy, X-ray diffraction (XRD), dynamic light scattering (DLS) with zeta potential and high resolution transmission electron microscopy (HR-TEM) with energy dispersive X-ray spectroscopy (EDS) analysis. The synthesized AgNPs were in the size range of 25–50 nm with a distorted spherical shape identified from HR-TEM analysis. The catalytic activity of AgNPs on the reduction of direct yellow-12 using NaBH4 was analyzed using a UV–Vis spectrophotometer. This study showed the efficacy of biogenic AgNPs in catalyzing the reduction of direct yellow-12.
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