扫描电子显微镜
傅里叶变换红外光谱
热液循环
材料科学
透射电子显微镜
微球
水热合成
化学工程
核化学
纳米技术
化学
复合材料
工程类
作者
Youzhi Liu,Youzhi Liu,Weizhou Jiao,Lixin Zhang
出处
期刊:Micro & Nano Letters
[Institution of Electrical Engineers]
日期:2010-01-01
卷期号:5 (5): 278-278
被引量:4
标识
DOI:10.1049/mnl.2010.0123
摘要
This Letter provides a template method to fabricate SiO2/β-Ni(OH)2 core/shell particles and hollow Ni(OH)2 microspheres through a hydrothermal process without any surface modifier. Hollow Ni(OH)2 microspheres with plicate surface are obtained after a SiO2 template is dissolved in the absence of NaOH. Experiments that differ in synthetic conditions are carried out to help in understanding the forming mechanism. The SiO2/β-Ni(OH)2 core/shell particles and hollow microspheres are characterised through X-ray diffraction (XRD), Fourier-transform infrared (FTIR), transmission electron microscopy (TEM) and scanning electron microscopy (SEM). The XRD and FTIR analyses indicate that the silica core is removed. SEM and TEM images confirm that Ni(OH)2 microspheres are hollow structured.
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