乙酸乙酯
葡聚糖
化学
硅胶
色谱法
柱色谱法
化学成分
有机化学
酶
出处
期刊:Chinese Journal of Experimental Traditional Medical Formulae
日期:2012-01-01
摘要
Objective:To study on chemical constituents of the ethyl acetate extract part of Stelmatocrypton khasianum.Method:Ethyl acetate extract part were isolated and pured by silica gel column chromatography,MCI and Sephadex LH-20,Their chemical structures were elucidated by spectral data analysis(1H-NMR and13C-NMR).Result:Five compounds were isolated from the ethyl acetate extract part,they were identified as syringaresinol(Ⅰ),diasyringaresinol(Ⅱ),episyringaresinol(Ⅲ),justiciresinol(Ⅳ),threo-4′,4″,7″,9″-tetrahydroxy-3,3′,3″,5-tetramethoxy-4,8″-oxy-7,9′∶ 7′,9-diepoxylignan(Ⅴ).Conclusion:Five kinds of compounds were isolated from S.khasianum for the first time.
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