葡聚糖
硅胶
化学
化学成分
色谱法
甲醇
乙酸乙酯
高效液相色谱法
碳-13核磁共振
光谱分析
有机化学
酶
光谱学
量子力学
物理
出处
期刊:China journal of Chinese materia medica
[China Journal of Chinese Materia Medica]
日期:2013-10-15
标识
DOI:10.4268/cjcmm20132023
摘要
To study the chemical constituents from the leaves of Aglaia testicularis. The methanol extract was isolated and purified by silica gel, Sephadex LH-20 and preparative HPLC. Their chemical structures were elucidated by MS and spectral data (1H, 13C-NMR). Seven compounds were isolated from the leaves and identified as dasyclamide (1), aglamide A (2), aglamide B (3), aglamide C (4), aglamide D (5), aglaroxin A 1-O-acetate (6), and 3'-methoxyaglaroxin A 1-0-acetate (7). All compounds were isolated from this plant for the first time.
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