试剂
杂原子
溶解度
化学
芳基
烷基
元素分析
水分
惰性气体
惰性
有机化学
核化学
作者
Jun Young Choi,Scott E. Denmark
标识
DOI:10.1002/047084289x.rn00825
摘要
[2351-34-0] C4H9ClSi (MW 120.65) InChI = 1S/C4H9ClSi/c1-6(5)3-2-4-6/h2-4H2,1H3 InChIKey = JWKKXHBGWAQZOK-UHFFFAOYSA-N (synthesis of alkyl, aryl, and heteroatom-substituted siletanes) Physical Data: bp 103 °C; d 0.985 g cm−3. Solubility: soluble in most aprotic organic solvents. Form Supplied in: colorless liquid. Analysis of Reagent Purity: elemental analysis, IR, M.S., NMR. Preparative Methods: siletane 1 can be prepared in large quantities by Wurtz coupling reaction of dichloro-3-chloropropylmethylsilane with Mg.1 It is commercially available from Gelest and Aldrich chemical company. Handling, Storage, and Precautions: moisture sensitive and corrosive; store under an inert atmosphere; use in a fume hood.
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