材料科学
锆钛酸铅
四方晶系
马弗炉
微晶
钙钛矿(结构)
钛酸铅
粒径
化学工程
相(物质)
矿物学
分析化学(期刊)
冶金
铁电性
化学
色谱法
催化作用
电介质
有机化学
工程类
光电子学
煅烧
作者
Darmawan Hidayat,Mohammad Taufik,Setianto Setianto
出处
期刊:Heliyon
[Elsevier]
日期:2022-03-01
卷期号:8 (3): e09125-e09125
被引量:9
标识
DOI:10.1016/j.heliyon.2022.e09125
摘要
This study aims to determine the one-step synthesis of lead zirconate titanate (PbZr(1-x)TixO3; PZT) particles, using a solid-state reaction method. These particles were synthesized at x of 0.48, using a solid-state reaction (SSR) method at various operating temperatures of 700-1000 °C. Before the reaction in a muffle furnace, the precursor powder was shaker milled for 2 h. The structural analysis of the diffraction patterns showed the formation of the PZT perovskite particles. It also showed the evolution from the tetragonal phase (at 800 and 900 °C) to the coexistence of tetragonal and rhombohedral stages in samples synthesized at 1000 °C. Furthermore, the crystallite particle size synthesized and commercialized at 1000 °C were 36.00 and 47.98 nm, respectively. These showed the formation of monodispersed size distribution, with an average of approximately 4.7 μm. Therefore, the PZT particles were successfully synthesized through a one-step synthesis, using the SSR method with a pre-mixed shaker milling.
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