This edition presented to your attention highlights the latest research results in the field of synthesis of materials and the study of their properties. The features of the synthesis are considered, and the properties of metal-organic frameworks, multifunctional nanocomposites, oxide nanostructures in electronics and optoelectronics, drug delivery systems in the treatment of oncological diseases and biocompatible coatings for implantology, as well as composites with a titanium matrix and the protective properties of a special cladding of structural steels and alloys, are studied. This edition will be helpful to a wide range of specialists in modern materials science.