Controlled Synthesis of NiCoP/g‐C3N4 Heterostructured Hybrids for Enhanced Visible‐Light‐Driven Hydrogen Evolution

Abstract An innovative system of graphitic C 3 N 4 with NiCoP as two‐component heterostructured hybrids (NiCoP/g‐C 3 N 4 ) with efficiently photocatalytic performances for hydrogen production is demonstrated and a simple, morphologically controlled catalyst with an extremely low phosphide load was developed. The hydrogengenerate rate is 1067.11 μmol g −1 h −1 using 1 ωt% NiCoP/g‐C 3 N 4 . The incorporation of monodisperse NiCoP nanoparticles into g‐C 3 N 4 effectively optimizes the electronic structures of the hybrids, enhances the corresponding interaction and the activity of hydrogen catalytic site, Moreover,NiCoP/g‐C 3 N 4 Heterostructured Hybrids displayed the favorable stability during the photocatalytic.